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Smoltek Hydrogenated AGC at the Smoltek office

Smoltek Hydrogen has finalized design of a Prototype Coater tool for carbon nanofibers

Smoltek Hydrogen and AGC Plasma Technology Solutions have finalized the design of a Prototype Coater for industrial growth of carbon nanofibers. The purpose with the tool is to verify that the nanofibers can be grown using a Plasma Enhanced Chemical Vapor Deposition (PECVD) technology from AGC. The technology is scalable and can be extended to be used for substrates of several square meters, for future mass production.

May 28, 2024

Smoltek Hydro­gen is work­ing on solv­ing the biggest pain point of PEM elec­trolyz­ers – “The Irid­i­um prob­lem”. Irid­i­um is need­ed as cat­a­lyst on the anode side in an elec­trolyz­er cell. How­ev­er, irid­i­um is extreme­ly expen­sive and most of all scarce and a lim­it­ed resource, and the short­age of irid­i­um is rec­og­nized as the sin­gle most severe threat towards scal­ing up PEM elec­trolyz­ers. For this rea­son, the hydro­gen indus­try is eager to find a new, game-chang­ing tech­nol­o­gy that can sig­nif­i­cant­ly reduce the irid­i­um load. 

Smoltek Hydro­gen has a solu­tion to this par­tic­u­lar prob­lem, by intro­duc­ing an ultra-thin irid­i­um coat­ing on the porous trans­port lay­er side instead of the mem­brane, and where the sur­face area first has been enlarged by coat­ing the sur­face with cor­ro­sion pro­tect­ed ver­ti­cal car­bon nanofibers.
Smoltek Hydro­gen aims to reduce the irid­i­um amount with 95% com­pared to today’s stan­dard mate­r­i­al (that uses ca 2.5 mg iridium/​cm2), and has recent­ly com­plet­ed a 1,000 hour dura­bil­i­ty test with only 0.2 mg iridium/​cm2 (Read about the test).

Man­u­fac­tur­ing tech­nolo­gies to enable scale-up of PEM elec­trolyz­ers
Besides hav­ing a game chang­ing tech­nol­o­gy, Smoltek Hydro­gen also need to be able to man­u­fac­ture the elec­trolyz­er cell mate­r­i­al in large vol­umes. Today the sam­ples are pro­duced with lab­o­ra­to­ry tech­nolo­gies, in low quan­ti­ties and with typ­i­cal area of only a few square cen­time­ters, where­as the indus­tri­al man­u­fac­tur­ing con­cept must be scal­able to the high vol­umes fore­seen, which is tens of thou­sands of square meters a year, and beyond. 

An impor­tant first step towards indus­tri­al­iza­tion and com­mer­cial­iza­tion of the Smoltek Hydro­gen elec­trolyz­er cell mate­r­i­al is prac­ti­cal val­i­da­tion of the select­ed con­cept for the growth of nanofibers, since it is a dif­fer­ent type of Plas­ma Enhanced Chem­i­cal Vapor Depo­si­tion (PECVD) process than used today. In order to do this Smoltek Hydro­gen has, togeth­er with AGC Plas­ma Tech­nol­o­gy Solu­tions, designed a new ded­i­cat­ed Pro­to­type Coater tool that will be placed in the Chalmers MC2 facil­i­ties in Gothen­burg, where Smoltek cur­rent­ly has its nanofiber fab­ri­ca­tion operations.

Smoltek Agc Tool Design
Ilus­tra­tion of the Pro­to­type Coater which has been designed in col­lab­o­ra­tion with AGC Plas­ma Tech­nol­o­gy Solu­tions. The Pro­to­type Coater shall be used to val­i­date the scal­able high-vol­ume man­u­fac­tur­ing tech­nol­o­gy for growth of car­bon nanofibers.

The Pro­to­type Coater is a pow­er­ful tool with small foot­print and will pro­vide an impor­tant plat­form for con­tin­ued devel­op­ment of indus­tri­al growth recipes. The ambi­tion with the tool is to com­bine scal­able AGC lin­ear hol­low cath­ode PECVD tech­nol­o­gy and our exper­tise in grow­ing car­bon nanofibers. We fine tune dif­fer­ent growth con­di­tions and select the para­me­ters most suit­able for fur­ther scale-up. The tool will also enable us to man­u­fac­ture rep­re­sen­ta­tive sam­ples to cus­tomers with indus­tri­al scal­able technology.

Shafiq Kabir, Head of Vol­ume Process­es at Smoltek Hydrogen

Based on the learn­ings from val­i­da­tion of the Pro­to­type Coater, Smoltek Hydro­gen aims to order a Pilot Coater, which is a small­er ver­sion of a high-vol­ume tool. This is also a cru­cial com­po­nent of AGC’s busi­ness mod­el, since they guar­an­tee the per­for­mance of the vol­ume machine if their small­er coater is used to spec­i­fy its require­ments. The Pilot Coater will be used to pro­duce test series for cus­tomers as well as for ver­i­fi­ca­tion of the pro­duc­tion tech­nolo­gies before vol­ume manufacturing.

Smoltek Manufacturing Strategy 2024 04
The roadmap for scal­ing up pro­duc­tion of Smoltek Elec­trolyz­er Cell Mate­r­i­al is per­formed in sev­er­al phas­es. The val­i­da­tion of the select­ed con­cept for the growth of nanofibers in the Pro­to­type Coater is an impor­tant first step in the indus­tri­al­iza­tion & com­mer­cial­iza­tion phase.

About AGC
AGC Plas­ma Tech­nol­o­gy Solu­tions is a new busi­ness unit with­in AGC Glass Europe SA, a Euro­pean leader in flat glass. AGC Plas­ma Tech­nol­o­gy Solu­tions is pro­vid­ing low-pres­sure plas­ma coat­ing tech­nol­o­gy and equip­ment. AGC Plas­ma is an expan­sive team of plas­ma coat­ing experts spe­cial­ized in inno­v­a­tive PVD and PECVD appli­ca­tions from R&D and new prod­uct devel­op­ment all the way through to equip­ment man­u­fac­tur­ing and oper­a­tional man­age­ment of mass pro­duc­tion coat­ing plants. Vis­it the web­site www.agc-plasma.com to learn more about the equip­ment and ser­vices offered by AGC Plas­ma Tech­nol­o­gy Solutions.

Peo­ple pic­tured in the top pho­to, from left: Amin Saleeem, Bastien Pen­ninckx, Shafik Kabir, Erwan-Axel Mor­ris­son (AGC), Fabi­an Wenger, Jeroen Schot­saert (AGC), Elli­nor Ehrn­berg, Réka Simon-Balint.

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